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Ingmand Laboratory at Ashland University


The Robert D. Ingmand Laboratory houses our analytical instrumentation.

Spectroscopy
Atomic Absorption Spectrometer
Fourier Transform Infrared Spectrometer
Spectrofluorophotometer
Ultraviolet/visible Spectrometer
Nuclear Magnetic Resonance

Chromatography
Capillary Electrophoresis
Gas Chromatography (GCMS)
Gas Chromatography (FID & EC)
Gas Chromatography (FID & TC)
Ion Exchange Chromatography
High Performance Liquid Chromatography

Misc
MALDI
Differential Scanning Calorimeter


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instrument lab
instrument lab
Atomic Absorption Spectrometer
SpectrAA 220FS (Varian)
Equipped with Graphite Furnace, Autosampler, SIPS, and VGA

This instrument is used to detect metals in samples at a concentration of 1 part per million and lower. 
 
    

List of Instruments


AA
Fourrier Transform Infrared Spectrometer
Perkin Elmer 16 PC

This instrument detects a molecule's absorption of infrared light.  Infrared light causes molecules to vibrate.  This instrument is used to determine a molecule's structure and identity based on the types of vibrations the molecule possesses.
     

List of Instruments


FTIR
Ultraviolet / Visible Spectrometer
Perkin Elmer Lambda 2

This instrument is used to measure the absorption of visible and ultraviolet light.  Molecules absorb these wavelengths of light and undergo electronic excitation. 
 
 

List of Instruments


UV
Spectrofluorimeter
Shimadzu RF 5301 PC

This instrument is used to measure the emmision of visible and ultraviolet light from molecules that have been optically excited to electronic excited states.  Molecules emit light when they make transitions from excited states to the ground electronic state. 
 

List of Instruments


fluorescence
Nuclear Magnetic Resonance

This instrument is used to determine the chemical structure of  molecules. It aids in the determination of hydrogen and carbon attachments in molecules.
 

List of Instruments     


nmr
Capillary Electrophoresis
Lumex Capel 103R

This Instrument is used to separate molecules in a capillary based on their size and the electrical charge that they posses.
 
   

List of Instruments


CE


Gas Chromatography (Mass Spectrometer Detector)
Hewlett Packard HP6890 GCMS

This instrument separates molecules based on their polarity and boiling point.  It detects the separated molecules by analyzing the mass of each component.
 
 
    

List of Instruments


GCMS
Gas Chromatography (flame ionization and electron capture detectors)
Perkin Elmer Autosystem

This instrument separates molecules based on their polarity and boiling point.  The electron capture detector enables the detection of halogenate molecules.
 
   

List of Instruments


gc
Gas Chromatography (flame ionization and thermal conductivity detectors)
Shimadzu GC 14A

This instrument separates molecules based on their polarity and boiling point.  It is used for preparative GC (separating molecules without destroying them so that they can be used in subsequent experiments).
   

List of Instruments


GC
Ion Exchange Chromatography
Dionex 

This instrument separates molecules based on the electrical charge that they posses.  It detects the molecules by electrochemical and conductivity detection.
 
      
   

List of Instruments


IC
High Performance Liquid Chromatography
Agilent 1100 Series
Equipped with diode array and refractive index detectors <>This instrument separates aqueous molecules based on size, molecular weight, polarity, and charge. It detects the separated molecules by examining the visible and ultraviolet absorption of the molecules or by detecting the refractive index of the molecules.
 
 
     
List of Instruments
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HPLC
Differential Scanning Calorimeter
Dupont (DSC 10)
Equipped with Thermal gravimetric analyzer (951 TGA)

This instrument measures the behavior of materials upon the addition of heat. It is used to identify molecules and characterize properties of polymers.
 
   

List of Instruments


dsc
Matrix Assisted Laser Desorption/Ionization
Bruker

This instrument is used to analyze biomolecules (biopolymers such as proteins, peptides and sugars) and large organic molecules (such as polymers, dendrimers and other macromolecules).
 
  




List of Instruments
MALDI


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